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• W2887615512 abstract "Defects of cyclotrimethylene trinitramine (RDX) crystals prepared by cooling crystallization in various mixed solvents were studied. A normal RDX and a reduced sensitivity RDX were compared with recrystallized RDX crystals in terms of thermal analysis by differential scanning calorimetry, matching refractive index, scanning electron microscopy, bulk density, and gas chromatography. Activation energy was calculated by thermal analysis using Kissinger’s plot and correlated with supersaturation, bulk density, and inclusion fraction. The quality of the RDX crystallized in various solvents was examined by the activation energy, which is expressed as a function of the supersaturation. Formation of crystals with smooth and flawed faces can be interpreted by the relationship between supersaturation and activation energy, which enables discrimination between a reduced sensitivity RDX and normal RDX. In high supersaturation, nucleation of new layers occurs at the edges and corners of the crystal, and layered growth becomes dominant. The cracks are characterized by the overlapping of layers at the crystal faces." @default.
• W2887615512 created "2018-08-22" @default.
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• W2887615512 date "2018-08-13" @default.
• W2887615512 modified "2023-09-23" @default.
• W2887615512 title "Quantitative Study on Crystal Defects Using the Relationship between Crystallization Parameters and Thermal Analysis" @default.
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• W2887615512 doi "https://doi.org/10.1021/acs.cgd.8b00453" @default.
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