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• W2890021797 abstract "There is significant interest in the development of process routes for active pharmaceutical ingredients using C–H arylation methodology. An efficient and practical synthetic route for febuxostat (1), which is the first non-purine-type xanthine oxidase inhibitor, was established via palladium- and copper-catalyzed C–H arylation of thiazole with aryl bromide. The catalyst loading was reduced to 0.1 mol % for the intermolecular C–H arylation, and a three-step synthesis produced febuxostat in 89% overall yield with excellent selectivity." @default.
• W2890021797 created "2018-09-27" @default.
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• W2890021797 date "2018-09-07" @default.
• W2890021797 modified "2023-09-29" @default.
• W2890021797 title "Process Development of Febuxostat Using Palladium- and Copper-Catalyzed C–H Arylation" @default.
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• W2890021797 doi "https://doi.org/10.1021/acs.oprd.8b00164" @default.
• W2890021797 hasPublicationYear "2018" @default.
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