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• W2890156334 abstract "Abstract In situ growth of metallic MoO 2 films on fluorine‐doped tin oxide (FTO) and MoO 2 powder in solution was achieved simultaneously by a simple hydrothermal process employing citric acid as the surfactant. The growth mechanism of MoO 2 nanostructures (NSs) at the heterogeneous interface and in homogeneous medium proceeds in a different manner in which seeds grow in a preferred orientation on FTO, whereas they propagate in all directions in solution. The high lattice matching of FTO and MoO 2 favours the film growth which could not be obtained on other conventional substrates. The disc morphology of MoO 2 nanostructures was changed to other diverse morphology by varying the synthesis conditions, particularly by the addition of nitric acid. A competitive effect of nitric acid and citric acid on the structure direction produced various shapes. The electrochemical water activation studies show that hydrogen‐annealed MoO 2 is an excellent hydrogen evolution reaction (HER) catalyst with good stability. H‐MoO 2 film/FTO displays a low onset overpotential of72 mV with a Tafel slope of 84.1 mV dec −1 , whereas the powder form exhibits an onset overpotential of 46 mV with a Tafel slope of 71.6 mV dec −1 . The large active surface area, exposure of fringe facets of (110) and the lesser electrochemical charge‐transfer resistance offered by the hydrogen‐annealed MoO 2 NSs play a major role in the enhanced HER activity." @default.
• W2890156334 created "2018-09-27" @default.
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• W2890156334 date "2018-11-08" @default.
• W2890156334 modified "2023-10-15" @default.
• W2890156334 title "Designing Metallic MoO₂ Nanostructures on Rigid Substrates for Electrochemical Water Activation" @default.
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• W2890156334 doi "https://doi.org/10.1002/chem.201803570" @default.
• W2890156334 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30182524" @default.
• W2890156334 hasPublicationYear "2018" @default.
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