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- W2890331344 abstract "A single crystal X-ray diffraction study of the new compound [Rb([2.2.2]crypt)]2[Rb([18]crown−6)][HGe9]·4NH3 revealed the presence of the first protonated nine-atom germanide cluster [HGe9]3−. It forms from Rb4Ge9 in liquid ammonia, so that [Ge9]4− can be considered as the base and [HGe9]3− its formally conjugated acid. The H atom is attached to a germanium vertex atom of the basal square plane, as it is known for [RGe9]3− (R = C5H9, Mes, etc.) or [HE9]3− (E = Si, Sn). In addition, the proton could be located unambiguously in the Fourier difference map. [HGe9]3− also represents a nido cluster species with 22 cluster-bonding electrons, which can be considered the most stable structure for nine-atom cluster species for all group 14 elements." @default.
- W2890331344 created "2018-09-27" @default.
- W2890331344 creator A5007760849 @default.
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- W2890331344 date "2018-09-21" @default.
- W2890331344 modified "2023-10-18" @default.
- W2890331344 title "Crystal Structure of the Protonated Germanide Cluster [HGe9]3−" @default.
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- W2890331344 doi "https://doi.org/10.3390/cryst8100374" @default.
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