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- W2890437977 abstract "The work described in this paper is directed towards the electrosynthesis of TTFCl0,77 as spherical nanoparticles by using amphiphilic molecules, behaving as growth-controlling agents. The morphology and the size distribution of the particles were analyzed using transmission electron microscopy and the resulting powders were characterized by infrared and Raman spectroscopy along with X-ray diffraction. In the presence of dodecylamine, electron micrographs evidenced spherical and relatively well-dispersed nanoparticles exhibiting a mean diameter of about 10 nm. However, in the presence of N-octylfurfurylimine, a mixture of nanoparticles and sticks were formed. The best results in terms of smallness of particles size and narrowness size distribution were obtained in the presence of 1-octanamine, N-(2-thienylmethylene). Spherical nanoparticles exhibiting sizes in the 4–12 nm range with an average size of about 8 nm were observed. The nanoparticles powder exhibited a room temperature conductivity of about 0.01 S.cm–1." @default.
- W2890437977 created "2018-09-27" @default.
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- W2890437977 date "2018-11-01" @default.
- W2890437977 modified "2023-10-01" @default.
- W2890437977 title "Nanoparticles of tetrathiafulvalene chloride derivatives grown in the presence of amphiphilic molecules" @default.
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- W2890437977 doi "https://doi.org/10.1016/j.synthmet.2018.08.019" @default.
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