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- W2890536064 endingPage "e4549" @default.
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- W2890536064 abstract "Six diiron ethanedithiolate complexes containing benzoate ester have been synthesized and characterized. Treatment of the starting material [{μ-SCH2CH(CH2OH)S}Fe2(CO)6] (1) with benzoic acid in the presence of N,N′-dicyclohexylcarbodiimide and 4-dimethylaminopyridine afforded the benzoate ester-containing complex [{μ-SCH2CH(CH2O2CPh)S}Fe2(CO)6] (2) in 97% yield. Carbonyl substitution of complex 2 with a monophosphine ligand, such as triphenylphosphine, tris(2-methoxyphenyl)phosphine, tris(4-fluorophenyl)phosphine, isopropyldiphenylphosphine or cyclohexyldiphenylphosphine, in the presence of Me3NO⋅2H2O gave the derivatives [{μ-SCH2CH(CH2O2CPh)S}Fe2(CO)5L] (L = PPh3, 3; P(C6H4OCH3-2)3, 4; P(C6H4F-4)3, 5; Ph2PCH(CH3)2, 6; Ph2PC6H11, 7) in 66–95% yields. Complexes 2–7 were characterized using elemental analysis, spectroscopy and X-ray diffraction analysis. In addition, these complexes can catalyze the reduction of protons to H2 in the presence of weak acid HOAc under electrochemical conditions." @default.
- W2890536064 created "2018-09-27" @default.
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- W2890536064 date "2018-09-06" @default.
- W2890536064 modified "2023-10-14" @default.
- W2890536064 title "Electrocatalytic properties of diiron ethanedithiolate complexes containing benzoate ester" @default.
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- W2890536064 doi "https://doi.org/10.1002/aoc.4549" @default.
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