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• W2890623145 endingPage "166" @default.
• W2890623145 startingPage "160" @default.
• W2890623145 abstract "In this research, electrochemical oxidation of acetaminophen was investigated in the presence of steroidal anti-inflammatory drugs diclofenac and piroxicam by cyclic voltammetry and controlled-potential coulometry techniques. The results indicated that N-acetyl-p-benzoquinone-imine (NAPQI), produced by electrooxidation of acetaminophen, reacts with diclofenac and piroxicam, via the Michael addition reaction. Corresponding products were electrochemically synthesized in aqueous solutions using a carbon electrode in an undivided cell. These products were identified by spectroscopic methods (FT-IR, 1HNMR, 13CNMR and MS). The homogeneous rate constants (kobs), based on the suggested electrode mechanism (i.e. EC), were estimated by comparing the experimental cyclic voltammetric responses with those digital simulated results. A comparison of the estimated kobs for the reaction of electrochemically generated N-acetyl-p-benzoquinone-imine (NAPQI) with steroidal anti-inflammatory drugs revealed that kobs (piroxicam) > kobs(diclofenac) at biological pH." @default.
• W2890623145 created "2018-09-27" @default.
• W2890623145 creator A5031448918 @default.
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• W2890623145 date "2018-10-01" @default.
• W2890623145 modified "2023-10-11" @default.
• W2890623145 title "Electrochemical oxidation of acetaminophen in the presence of diclofenac and piroxicam - Synthesis of new derivatives and kinetic investigation of toxic quinone imine/drugs interactions" @default.
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• W2890623145 doi "https://doi.org/10.1016/j.jelechem.2018.09.021" @default.
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