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• W2890729425 endingPage "11086" @default.
• W2890729425 startingPage "11078" @default.
• W2890729425 abstract "Sulfidated nanoscale zerovalent iron (S-nZVI) has the potential to be a cost-effective remediation agent for a wide range of environmental pollutants, including chlorinated solvents. Various synthesis approaches have yielded S-nZVI consisting of a Fe0 (or Fe0/S0) core and FeS shell, which are significantly more reactive to trichloroethene (TCE) than nZVI. However, their reactivity is not as high as palladium-doped nZVI (Pd-nZVI). We synthesized S-nZVI by the co-precipitation of FeS and Fe0 by using Na2S during the borohydride reduction of FeSO4 (S-nZVIco). This resulted in FeS structures bridging the nZVI core and the surface, as confirmed by electron microscopy and X-ray analyses. The TCE degradation capacity of up to 0.46 mol TCE/mol Fe0 was obtained for S-nZVIco at a high S loading and was comparable to Pd-nZVI but 60% higher than the currently most reactive S-nZVI, in which FeS only coats the nZVI (S-nZVIpost). The high TCE degradation was due to complete utilization of Fe0 (2 e–/mol Fe0) toward the formation of acetylene. Although Pd-nZVI yielded 3 e–/mol Fe0, TCE degradation was comparable because it reduced acetylene further to ethene and ethane. Under Fe0-limited conditions, the S-nZVIco TCE degradation rate was 16 times higher than that of Pd-nZVI (0.5 wt % Pd) and 90 times higher than that of S-nZVIpost." @default.
• W2890729425 created "2018-09-27" @default.
• W2890729425 creator A5030574495 @default.
• W2890729425 creator A5059886531 @default.
• W2890729425 date "2018-09-06" @default.
• W2890729425 modified "2023-10-16" @default.
• W2890729425 title "Optimal Design of Sulfidated Nanoscale Zerovalent Iron for Enhanced Trichloroethene Degradation" @default.
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• W2890729425 doi "https://doi.org/10.1021/acs.est.8b02399" @default.
• W2890729425 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30188121" @default.
• W2890729425 hasPublicationYear "2018" @default.
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