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• W2890947138 endingPage "2410" @default.
• W2890947138 startingPage "2404" @default.
• W2890947138 abstract "Copper(I)-promoted click cyclization in the presence of TBTA afforded nucleoside macrocycles in very high yields (≈70%) without using protecting groups. To this end, dU and dC derivatives functionalized at the 5-position of the nucleobase with octadiynyl side chains and with azido groups at the 5’-position of the sugar moieties were synthesized. The macrocycles display freely accessible Watson–Crick recognition sites. The conformation of the 16-membered macrocycle was deduced from X-ray analysis and 1 H, 1 H-NMR coupling constants. The sugar conformation ( N vs S ) was different in solution as compared to the solid state." @default.
• W2890947138 created "2018-09-27" @default.
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• W2890947138 date "2018-09-13" @default.
• W2890947138 modified "2023-09-30" @default.
• W2890947138 title "Nucleoside macrocycles formed by intramolecular click reaction: efficient cyclization of pyrimidine nucleosides decorated with 5'-azido residues and 5-octadiynyl side chains" @default.
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• W2890947138 doi "https://doi.org/10.3762/bjoc.14.217" @default.
• W2890947138 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6142766" @default.
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• W2890947138 hasPublicationYear "2018" @default.
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