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• W2890969118 endingPage "1122" @default.
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• W2890969118 abstract "The synthesis and characterization of two dinuclear complexes, namely fac -hexacarbonyl-1κ 3 C ,2κ 3 C -(pyridine-1κ N )[μ-2,2′-sulfanediyldi(ethanethiolato)-1κ 2 S 1 , S 3 :2κ 3 S 1 , S 2 , S 3 ]dirhenium(I), [Re 2 (C 4 H 8 S 3 )(C 5 H 5 N)(CO) 6 ], ( 1 ), and tetraethylammonium fac -tris(μ-2-methoxybenzenethiolato-κ 2 S : S )bis[tricarbonylrhenium(I)], (C 8 H 20 N)[Re 2 (C 7 H 7 OS) 3 (CO) 6 ], ( 2 ), together with two mononuclear complexes, namely (2,2′-bithiophene-5-carboxylic acid-κ 2 S , S ′)bromidotricarbonylrhenium(I), ( 3 ), and bromidotricarbonyl(methyl benzo[ b ]thiophene-2-carboxylate-κ 2 O , S )rhenium(I), ( 4 ), are reported. Crystals of ( 1 ) and ( 2 ) were characterized by X-ray diffraction. The crystal structure of ( 1 ) revealed two Re—S—Re bridges. The thioether S atom only bonds to one of the Re I metal centres, while the geometry of the second Re I metal centre is completed by a pyridine ligand. The structure of ( 2 ) is characterized by three S-atom bridges and an Re...Re nonbonding distance of 3.4879 (5) Å, which is shorter than the distance found for ( 1 ) [3.7996 (6)/3.7963 (6) Å], but still clearly a nonbonding distance. Complex ( 1 ) is stabilized by six intermolecular hydrogen-bond interactions and an O...O interaction, while ( 2 ) is stabilized by two intermolecular hydrogen-bond interactions and two O...π interactions." @default.
• W2890969118 created "2018-09-27" @default.
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• W2890969118 date "2018-09-13" @default.
• W2890969118 modified "2023-09-24" @default.
• W2890969118 title "Synthesis of Re^Itricarbonyl complexes with various sulfur- and oxygen-donating ligands: crystal structures of two Re^Idinuclear structures bridged by S atoms" @default.
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• W2890969118 doi "https://doi.org/10.1107/s205322961801207x" @default.
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