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- W2890972423 abstract "In the development of new pharmaceutical formulations it is important to consider the possible interactions between the active pharmaceutical ingredient (API) and excipients which is a well-known problem. The objective of the work presented here was to investigate such reactions by means of diffusion ordered NMR spectroscopy (DOSY). The known reaction of 5-aminosalicylic acid (5-ASA) and the excipient citric acid was studied. Three reaction products have been verified by DOSY, 1H NMR and HPLC measurements. Despite a poor separation in the DOSY diagram, the reaction products could be assign due to the processing of thoughtful selected parts of the signals. The reaction of 5-ASA with formic acid and benzocaine with dibutyl phthalate was also studied by means of DOSY experiments." @default.
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- W2890972423 date "2019-01-01" @default.
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- W2890972423 title "Diffusion ordered NMR spectroscopy measurements as screening method of potential reactions of API and excipients in drug formulations" @default.
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- W2890972423 doi "https://doi.org/10.1016/j.jpba.2018.09.020" @default.
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