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• W2890985984 abstract "The bis(trimethylsilyl)amido group {N(SiMe3)2}-1, 2 is one of the simplest, most versatile, and inexpensive bulky monodentate ligands. Its steric properties were first demonstrated by Bürger and Wannagat via the synthesis of several low- (i.e. two- or three-) coordinate transition metal derivatives in the early 1960s. The list of new compounds included the trivalent complexes M{N(SiMe3)2}3 (M = Cr and Fe), the divalent species M{N(SiMe3)2}2 (M = Mn, Co, and Ni (unstable)), and the monovalent Cu{N(SiMe3)2}. In essence, the improved synthetic characterization methods and readily available crystal handling techniques for X-ray crystallographic studies available to modern workers have permitted all of Bürger and Wannagat's originally reported metal bis silylamido compounds to be unambiguously characterized. The chapter describes in detail reliable synthetic procedures for the uncomplexed metal bissilylamides M{N(SiMe3)2}2 (M = Mn, Fe, or Co) as well as those of their mono-tetrahydrofuran complexes M{N(SiMe3)2}2(THF). It provides a synthesis for the bis(THF) complex Mn{N(SiMe3)2}2(THF)2." @default.
• W2890985984 created "2018-09-27" @default.
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• W2890985984 date "2018-09-07" @default.
• W2890985984 modified "2023-10-17" @default.
• W2890985984 title "DIVALENT MANGANESE, IRON, AND COBALT BIS(TRIMETHYLSILYL)AMIDO DERIVATIVES AND THEIR TETRAHYDROFURAN COMPLEXES" @default.
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• W2890985984 doi "https://doi.org/10.1002/9781119477822.ch1" @default.
• W2890985984 hasPublicationYear "2018" @default.
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