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- W2890988170 abstract "In this paper, a simple and reliable method has been established to determine the residues of nine pesticides in tobacco by using GC–MS coupled with magnetic solid phase extraction. A novel magnetic Zr-MOF nanocomposite based on graphene was synthesized, and characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier-transform infrared spectroscopy (FT-IR), Raman spectroscopy and N2 adsorption-desorption measurements. The prepared material has the advantage of large surface area (178 m2/g), good magnetic response and high thermal stability, which is shown to be suited for the fast enrichment of multi-pesticides in tobacco matrix. The extraction conditions including amount of adsorbent, adsorption time, eluting solvent as well as desorption time were investigated. The whole process of pretreatment is accomplished within 10 min. This method shows low limit of detection, wide linear range and good reproducibility (relative standard deviations <12.7%), satisfactory recoveries were obtained, ranging from 57.9% to 126.3% for tobacco samples." @default.
- W2890988170 created "2018-09-27" @default.
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- W2890988170 date "2018-11-01" @default.
- W2890988170 modified "2023-10-05" @default.
- W2890988170 title "The synthesis of Zr-metal-organic framework functionalized magnetic graphene nanocomposites as an adsorbent for fast determination of multi-pesticide residues in tobacco samples" @default.
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- W2890988170 doi "https://doi.org/10.1016/j.chroma.2018.09.041" @default.
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