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• W2890988770 abstract "Late stage diversification of calix[4]arenes and thiacalix[4]arenes with heterocycles remains a significant synthetic challenge and hampers further exploitation of the scaffolds. Here we describe the development of a short and facile synthetic route to conformationally diverse novel calix[4]arene and thiacalix[4]arene ynones using a palladium cross coupling approach (5% Pd(ii) + 10% Cu(i)) with benzoyl chloride. Their successful conversion to heterocycles to afford pyrazoles was demonstrated through treatment with hydrazine. Functionalisation is calixarene conformation and linker independent enabling access to a library of structures." @default.
• W2890988770 created "2018-09-27" @default.
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• W2890988770 date "2018-01-01" @default.
• W2890988770 modified "2023-10-18" @default.
• W2890988770 title "Calixarene alpha-ketoacetylenes: versatile platforms for reaction with hydrazine nucleophile" @default.
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• W2890988770 doi "https://doi.org/10.1039/c8ra06349d" @default.
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