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- W2891245677 abstract "Abstract The polymeric organotin(IV) selenate complex [(Me 3 Sn) 3 (SeO 4 )(OH)] n ( 1 ) has been isolated as single crystals from the reaction of [(Me 2 NH 2 ) 2 SeO 4 ] and Me 3 SnCl in methanol. In the solid state, compound 1 was characterized by X-ray diffraction analysis, Fourier transform-infrared spectroscopy, and elemental analysis. 1 crystallizes in the orthorhombic system space group Pbca with a =11.0231(2) Å, b =16.3461(3) Å, c =20.9945(4) Å, α = β = γ =90°, V =3782.89(12) Å 3 , and Z =8. Its structure can be described as a polymeric zigzag chain based on Me 3 Sn moieties linked by tridentate selenate anions. Pendant (Me 3 Sn) 2 OH groups are also connected to the chain, according to a syndiotactic organization, and via Sn-O-Se bonds. Intermolecular OH···O hydrogen bonds and long Se-O···Sn distance interactions promote the association of chains together and lead to the propagation of a three-dimensional network. In addition, the behavior of 1 in solution (methanol) was also studied by multinuclear nuclear magnetic resonance spectroscopy and mass spectrometry." @default.
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- W2891245677 date "2018-11-27" @default.
- W2891245677 modified "2023-10-11" @default.
- W2891245677 title "Synthesis, spectroscopic study, and crystal structure of a new organotin(IV) selenate derivative" @default.
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- W2891245677 doi "https://doi.org/10.1515/mgmc-2018-0029" @default.
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