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- W2891403265 endingPage "12356" @default.
- W2891403265 startingPage "12334" @default.
- W2891403265 abstract "Azides are building blocks of increasing importance in synthetic chemistry, chemical biology, and materials science. Azidobenziodoxolone (ABX, Zhdankin reagent) is a valuable azide source, but its safety profile has not been thoroughly established. Herein, we report a safety study of ABX, which shows its hazardous nature. We introduce two derivatives, tBu-ABX and ABZ (azidobenziodazolone), with a better safety profile, and use them in established photoredox- and metal-mediated azidations, and in a new ring-expansion of silylated cyclobutanols to give azidated cyclopentanones." @default.
- W2891403265 created "2018-09-27" @default.
- W2891403265 creator A5008165586 @default.
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- W2891403265 creator A5087908327 @default.
- W2891403265 date "2018-09-15" @default.
- W2891403265 modified "2023-10-16" @default.
- W2891403265 title "Cyclic Hypervalent Iodine Reagents for Azidation: Safer Reagents and Photoredox-Catalyzed Ring Expansion" @default.
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- W2891403265 doi "https://doi.org/10.1021/acs.joc.8b02068" @default.
- W2891403265 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30220207" @default.
- W2891403265 hasPublicationYear "2018" @default.
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