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• W2891649541 abstract "Alumina supports were synthesized from aluminum hydroxide produced by the hydrolysis of secondary aluminum butoxide in the presence of the triblock copolymer Pluronic P123 (m-AlOOH) and from the commercial AlOOH pseudoboehmite powder (TH-AlOOH), as well as by mixing of m-AlOOH and TH-AlOOH gel in a ratio of 5:95 (m-TH-AlOOH sample). NiW/Al2O3 catalysts were prepared by impregnation of the synthesized supports with H3PW12O40 heteropolyacid and nickel citrate. Physicochemical properties of the supports and catalysts were investigated by low-temperature nitrogen adsorption, X-ray diffraction, NH3 thermo-programmed desorption, X-ray photoelectron spectroscopy, and high-resolution transmission electron microscopy. Catalytic properties were tested in hydrotreatment of straight-run gas oil and vacuum gasoil on a flow unit. The resulting hybrid support had a non-additively higher average pore radius (75 Å) and surface area (307 m2/g) than a conventional alumina support and hence preferred morphology of NiWS active phase (3.8 nm against 6.6 nm with the same stacking number) and an increase in the W sulfidation degree (68% against 54%) and Ni content in NiWS phase (44% against 26%). Therefore, the catalyst on the hybrid support exhibits higher activity in hydrodesulfurization, hydrodenitrogenation and hydrogenation of petroleum feeds, and a lower degree of deactivation and coke formation." @default.
• W2891649541 created "2018-09-27" @default.
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• W2891649541 date "2018-12-01" @default.
• W2891649541 modified "2023-10-18" @default.
• W2891649541 title "Influence of mesostructured alumina on the morphology of the active phase in NiWS/Al2O3 catalysts and their activity in hydrotreating of SRGO and VGO" @default.
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• W2891649541 doi "https://doi.org/10.1016/j.fuproc.2018.09.015" @default.
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