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- W2891833085 abstract "Synchrotron X-ray diffraction was used to monitor the hydrothermal precipitation of akaganeite ( β -FeOOH) and its transformation to hematite (Fe 2 O 3 ) in situ . Akaganeite was the first phase to form and hematite was the final phase in our experiments with temperatures between 150 and 200 °C. Akaganeite was the only phase that formed at 100 °C. Rietveld analyses revealed that the akaganeite unit-cell volume contracted until the onset of dissolution, and subsequently expanded. This reversal at the onset of dissolution was associated with a substantial and rapid increase in occupancy of the Cl site, perhaps by OH − or Fe 3+ . Rietveld analyses supported the incipient formation of an OH-rich, Fe-deficient hematite phase in experiments between 150 and 200 °C. The inferred H concentrations of the first crystals were consistent with “hydrohematite.” With continued crystal growth, the Fe occupancies increased. Contraction in both a- and c -axes signaled the loss of hydroxyl groups and formation of a nearly stoichiometric hematite." @default.
- W2891833085 created "2018-09-27" @default.
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- W2891833085 date "2018-09-10" @default.
- W2891833085 modified "2023-10-16" @default.
- W2891833085 title "Evolution in the structure of akaganeite and hematite during hydrothermal growth: an<i>in situ</i>synchrotron X-ray diffraction analysis" @default.
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- W2891833085 doi "https://doi.org/10.1017/s0885715618000623" @default.
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