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• W2892056070 abstract "N-Alkyl bis(2-selanylethyl)amines catalyze the synthesis of peptide thioesters or peptide ligation from bis(2-sulfanylethyl)amido (SEA) peptides. These catalysts are generated in situ by reduction of the corresponding cyclic diselenides by tris(2-carboxyethyl)phosphine. They are particularly efficient at pH 4.0 by accelerating the thiol-thioester exchange processes, which are otherwise rate-limiting at this pH. By promoting SEA-mediated reactions at mildly acidic pH, they facilitate the synthesis of complex peptides such as cyclic O-acyl isopeptides that are otherwise hardly accessible." @default.
• W2892056070 created "2018-09-27" @default.
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• W2892056070 date "2018-09-19" @default.
• W2892056070 modified "2023-10-01" @default.
• W2892056070 title "Catalysis of Thiol–Thioester Exchange by Water-Soluble Alkyldiselenols Applied to the Synthesis of Peptide Thioesters and SEA-Mediated Ligation" @default.
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• W2892056070 doi "https://doi.org/10.1021/acs.joc.8b01903" @default.
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