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- W2892322900 abstract "(1,1,2,2-Tetrafluorobut-3-en-1-yl)zinc bromide was prepared by insertion of the zinc-silver couple into the CF2-Br bond of commercially available 4-bromo-3,3,4,4-tetrafluorobut-1-ene in DMF at 0 °C for 0.5 h, The resultant polyfluorinated zinc reagent was found to be thermally stable at ambient temperature and storable for at least 1.5 years in the refrigerator. This CF2CF2-containing organozinc reagent could be easily transmetallated to copper species, which underwent cross-coupling reactions with various aromatic iodides or acyl chlorides to produce a broad range of CF2CF2-containing organic molecules in good-to-excellent yields. Therefore, the zinc reagent could become a new and practical synthetic tool for producing functional molecules with a CF2CF2 fragment." @default.
- W2892322900 created "2018-09-27" @default.
- W2892322900 creator A5054603118 @default.
- W2892322900 creator A5061320155 @default.
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- W2892322900 date "2018-09-11" @default.
- W2892322900 modified "2023-10-02" @default.
- W2892322900 title "Practical tetrafluoroethylene fragment installation through a coupling reaction of (1,1,2,2-tetrafluorobut-3-en-1-yl)zinc bromide with various electrophiles" @default.
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- W2892322900 doi "https://doi.org/10.3762/bjoc.14.213" @default.
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