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- W2892414405 abstract "The purpose of this study was to investigate the chemical stability and the mechanism of hydrolysis of the polyester wall of lipid-core nanocapsules (LNC) dispersed in water comparing sterile and non-sterile formulations. Sterile or non-sterile LNC formulations (LNCS and LNC, respectively) were prepared using poly(ε-caprolactone) (PCL) with different molar masses (Mn 10 kg mol−1, Mn 80 kg mol−1 and a mixture (1:9, w/w) of both PCL). All formulations presented unimodal size distribution profile without significant changes (p > .05) after 60 days. Molar weight changes, fraction of chain scissions and hydrolysis mechanism of LNC under storage (60 days; 5 °C) were determined by size exclusion chromatography (SEC). The highest PCL weight loss was observed for the non-sterile formulations (LNC 1–45%; LNC 2–32%; LNC 3–27%). In turn, the sterile formulations showed a lower weight loss, proving that biotic hydrolysis was responsible for accelerating hydrolysis of the LNC even when stored at low temperature (5 °C). In conclusion, the predominant hydrolysis mechanism was of the non-catalyzed type." @default.
- W2892414405 created "2018-10-05" @default.
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- W2892414405 date "2018-12-01" @default.
- W2892414405 modified "2023-10-03" @default.
- W2892414405 title "Chemical stability, mass loss and hydrolysis mechanism of sterile and non-sterile lipid-core nanocapsules: The influence of the molar mass of the polymer wall" @default.
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- W2892414405 doi "https://doi.org/10.1016/j.reactfunctpolym.2018.09.018" @default.
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