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• W2892967355 abstract "Abstract By using deep eutectic solvent mixture of ChCl (ChCl = choline chloride) and 1,8-diaminooctane as reaction medium, three new selenidostannates were synthesized, namely [Cr(en)3]2.5[SnSe4]·Cl3.5·(pip)0.5·1.5H2O (1) (en = ethylenediamine, pip = piperazine), [Ni(en)3][Sn3Se6.5(Se2)0.5] (2), and [Ni(en)3][Sn3Se7] (3). Compound 1 features a primary unit of SnSe4 tetrahedron, in which the [Cr(en)3]3+ complex acts as charge balance agent. In compound 2, there are two kinds of one dimensional chains, including [Sn3Se7]n2n– and [Sn3Se6(Se)2]n2n– anionic chains. The [Sn3Se7]n2n– chain is constructed by connecting [Sn3Se9] units via edge-sharing Se2- ion, while the [Sn3Se6(Se)2]n2n– chain is constructed by linking [Sn3Se10] units via sharing one Se2- ion and one Se22- ion. Compound 3 features a lamellar anionic [Sn3Se7]n2n– structure, where the [Ni(en)3]2+ ions are located in inter-lamellar space. The optical absorption spectra indicate band gaps of 2.23 eV for 1, 1.95 eV for 2, and 2.01 eV for 3." @default.
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• W2892967355 date "2019-01-01" @default.
• W2892967355 modified "2023-10-16" @default.
• W2892967355 title "Growing crystalline selenidostannates in deep eutectic solvent" @default.
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• W2892967355 doi "https://doi.org/10.1016/j.ica.2018.09.046" @default.
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