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• W2893284996 abstract "Abstract Chloro(pentafluorophenoxy)triphenylantimony Ph3SbCl(OC6F5) (3a) and chloro(pentachlorophenoxy)triphenylantimony Ph3SbCl(OC6Cl5) (3b) were synthesized by the reactions of triphenylantimony dichloride (1) with bis(pentafluorophenoxy)triphenylantimony (2a) and bis(pentachlorophenoxy)triphenylantimony (2b), respectively. The structure of compounds 3a,b was confirmed by IR, 1H, 13C{1H} and 19F{1H} NMR spectroscopy, elemental analysis and single-crystal X-ray diffraction study. According to X-ray diffraction data, two types of crystallographically independent molecules exist in crystals 3a and 3b. The antimony atoms have a distorted trigonal bipyramidal coordination with the chlorine and oxygen atoms in axial positions. The axial OSbCl angles in 3a and 3b are 177.07(19)°, 177.09(19)° and 178.25(5)°, 178.28(5)°, respectively; the equatorial angles are 118.0(9)о―122.2(4)° (3a) and 113.49(8)о―129.23(8)° (3b). The Sb―C equatorial bond lengths are 2.090(11)―2.136(9) A (3a), 2.099(2)―2.119(2) A (3b), and the Sb―Cl axial bond lengths are 2.464(4), 2.466(4) A (3a), 2.4920(10), 2.4912(9) A (3b). The Sb―O bond lengths are 2.102(7), 2.092(7) A (3a) and 2.0922(16), 2.0910(16) A (3b)." @default.
• W2893284996 created "2018-10-05" @default.
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• W2893284996 date "2018-12-01" @default.
• W2893284996 modified "2023-09-24" @default.
• W2893284996 title "Synthesis and structure of chlorotriphenylantimony pentafluoro- and pentachloroaroxides" @default.
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• W2893284996 doi "https://doi.org/10.1016/j.jfluchem.2018.09.005" @default.
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