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• W2893460870 abstract "A strategy for the preparation of silica-based monolithic capillary columns (150 × 0.1 mm) with high selectivity to amino acids is presented. The zwitterionic columns were prepared by coating the silica monolith with [2-(methacryloyloxy)ethyl]-dimethyl-(3-sulfopropyl)-ammonium hydroxide via 3-(trimethoxysilyl)propyl methacrylate. The columns were evaluated under isocratic conditions in hydrophilic interaction liquid chromatography. The best separation of amino acids was obtained on the monolithic column prepared by a stepwise modification procedure where the modification step was repeated four times. The mixture of fifteen amino acids was separated within 13 min using the mobile phase consisting of 75% acetonitrile and 25% 5 mmol/L ammonium acetate at pH 4.5." @default.
• W2893460870 created "2018-10-05" @default.
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• W2893460870 date "2018-10-02" @default.
• W2893460870 modified "2023-10-01" @default.
• W2893460870 title "Monolithic Silica Capillary Columns with Improved Retention and Selectivity for Amino Acids" @default.
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• W2893460870 doi "https://doi.org/10.3390/separations5040048" @default.
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