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• W2894326222 abstract "Abstract Large- and extra-large-pore zeolites have potential use in catalytic conversions of large molecules and thus attracted great attention in the fields of materials chemistry, catalysis and industry. In this study, a large-pore germanosilicate zeolite ITQ-26 with intersecting 12 × 12 × 12 pores was prepared by using an easily-obtained organic cation 1,2-dimethyl-3-(2-fluorobenzyl)-imidazolium or 1-methyl-3-(2-fluorobenzyl)-imidazolium as a structure-directing agent (SDA). The prepared ITQ-26 was characterized by means of synchrotron radiation, X-ray powder diffraction, thermogravimetric analysis, liquid and solid 13C/19F/29Si MAS NMR, photoluminescence spectroscopy, and N2 sorption analyses. Compared to those prepared by using phosphonium cations as SDAs, ITQ-26 prepared in this work has a larger Brunauer–Emmett–Teller (BET) surface area and pore volume. The germanium in ITQ-26 could be partially substituted by silicon during the post-synthetic modification treatment. Furthermore, it is shown that, like several recently-reported large- and extra-large-pore zeolites such as NUD-1, NUD-2, ITQ-37, ITQ-29, etc., the organic cations in the synthetic gel likely self-assemble into supramolecules, which act as structure-direction agents in the formation of ITQ-26. This work not only provides a facile method to prepare ITQ-26, but also demonstrates a potentially general, and useful approach to prepare new large and extra-large pore zeolites." @default.
• W2894326222 created "2018-10-05" @default.
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• W2894326222 date "2019-03-01" @default.
• W2894326222 modified "2023-10-18" @default.
• W2894326222 title "Facile synthesis of large-pore zeolite ITQ-26 by using an easily-available imidazolium as structure-directing agent" @default.
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• W2894326222 doi "https://doi.org/10.1016/j.micromeso.2018.09.022" @default.
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