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- W2894474448 abstract "An efficient and transition-metal-free method for the synthesis of the structurally diversified trifluoroethylthiol phenanthridines and 3,4-dihydroisoquinolines is described. Various 2-isothiocyanobiaryls and aryl alkyl isothiocyanates reacted with phenyl(2,2,2-trifluoroethyl)iodonium triflate in CH2Cl2 in the presence of trifluoromethanesulfonic acid at 40 °C to form the corresponding trifluoroethylation/cyclization products in good to quantitative yields. This work represents the first construction of trifluoroethylthiol phenanthridine and isoquinoline derivatives from isothiocyanates in the absence of transition-metal catalysts by a one-pot procedure." @default.
- W2894474448 created "2018-10-05" @default.
- W2894474448 creator A5068902661 @default.
- W2894474448 creator A5071393929 @default.
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- W2894474448 date "2018-09-28" @default.
- W2894474448 modified "2023-09-27" @default.
- W2894474448 title "TfOH-Promoted Transition-Metal-Free Cascade Trifluoroethylation/Cyclization of Organic Isothiocyanates by Phenyl(2,2,2-trifluoroethyl)iodonium Triflate" @default.
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- W2894474448 doi "https://doi.org/10.1021/acs.orglett.8b02793" @default.
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