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- W2894885993 abstract "Cinnamon bark is a very complex spices matrix for pesticide residue analysis. In this study, two cleanup procedures, dispersive solid-phase extraction (d-SPE) and repetitive d-SPE, combined with Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction were both investigated and applied for the determination of 60 pesticide residues in cinnamon bark by liquid chromatography − tandem mass spectrometry (LC-MS/MS) detection. The extraction solvents, phase partition salts, and cleanup sorbents were optimized. The results showed that 150 mg MgSO4 + 50 mg C18 showed the best performance in d-SPE. The repetitive d-SPE achieved less matrix effects than d-SPE, but several high water-solubility analytes were lost during the cleanup, and also the 10 fold dilution compromised the sensitivities of analytes. With the validated QuEChERS-d-SPE method, 44 of 60 pesticides obtained satisfactory recoveries (71%–118%) and RSDs (2%–27%) at three to five spiking levels. The method was applied to monitor 15 market cinnamon samples." @default.
- W2894885993 created "2018-10-12" @default.
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- W2894885993 date "2019-03-01" @default.
- W2894885993 modified "2023-10-11" @default.
- W2894885993 title "Evaluation of cleanup procedures in pesticide multi-residue analysis with QuEChERS in cinnamon bark" @default.
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- W2894885993 doi "https://doi.org/10.1016/j.foodchem.2018.10.019" @default.
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