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• W2894904556 abstract "n-Heptanol bearing a long hydrocarbon chain is for the first time attempted as poor solvent for reprecipitation of fullerene C60 crystals, which unprecedentedly prompts the selective synthesis of well-faceted parallelepiped, hexagonal plate, cuboctahedron, octahedron C60 crystals, as well as their derivatives with varying degrees of edge- and corner-truncation. Our comprehensive investigations support that morphology evolution is systematically modulated by the solvent proportion of n-heptanol, where increasing the proportion of n-heptanol gradually tunes C60 growth behavior from thermodynamic to kinetic regime, and thus induces a general shape evolution from parallelepiped or truncated parallelepiped, to an intermediate shape like hexagonal plate or truncated octahedron or cuboctahedron, eventually into octahedron. We also prove the existence of n-heptanol molecules as high as 10 wt % inside the final C60 polyhedral crystals, which results in the extraordinarily PL enhancement as well as an obvious blue-shift of PL peaks when compared to that of the solvent-free crystal. Our study provides a fundamental understanding toward the solvent-mediated shape-control process for organic polyhedral crystals, enlightening on solvent-intercalate-induced unique properties." @default.
• W2894904556 created "2018-10-12" @default.
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• W2894904556 date "2018-10-01" @default.
• W2894904556 modified "2023-10-15" @default.
• W2894904556 title "Solvent-Mediated Shape Engineering of Fullerene (C₆₀) Polyhedral Microcrystals" @default.
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• W2894904556 doi "https://doi.org/10.1021/acs.chemmater.8b03095" @default.
• W2894904556 hasPublicationYear "2018" @default.
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