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• W2895076212 abstract "The first enantioselective total synthesis of JBIR-03 and asporyzin C, indole diterpenoids of fungal origin exhibiting a range of pharmacologically important biological activities, has been accomplished from a known bicyclic keto alcohol in 13 and 14 steps, respectively. A hydroxy-directed cyclopropanation and Pd(II)-mediated indole ring formation were exploited as the key steps to obtain a pivotal pentacylic intermediate, which was converted into asporyzin C via chain elongation using cross-metathesis and then into JBIR-03 by Pd(II)-catalyzed tetrahydrofuran ring formation in an exclusively diastereoselective manner." @default.
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• W2895076212 date "2018-11-01" @default.
• W2895076212 modified "2023-10-09" @default.
• W2895076212 title "Total synthesis of JBIR-03 and asporyzin C" @default.
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• W2895076212 doi "https://doi.org/10.1016/j.tetlet.2018.10.009" @default.
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