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- W2895525880 abstract "To gain understanding of how the variation in local weak interactions influences intermolecular interactions and subsequent crystal packing, four analogues of 2-(3-chloro-2-methyl-phenylamino)-nicotinic acid [clonixin] were synthesized by replacing the chlorine with fluorine (1), bromine (2), iodine (3), and hydrogen (4). Compounds 1, 2, and 3 were found to be polymorphic as shown by the discovery of two forms for each (1-I, 1-II; 2-I, 2-II; and 3-I, 3-II, respectively), while compound 4 has only a single identified form. Similar to clonixin, the analogue molecules in their crystals are associated either by the acid–acid dimer homosynthon or the acid–pyridine heterosynthon, depending on the dihedral angle between the two aromatic rings. Moreover, forms 2-I, 2-II, 3-I, and 3-II are isostructural to clonixin forms I and IV, compound 4 is isostructural to compound 1 form I, and 2-II is structurally similar to clonixin form II. The phase behaviors of these polymorphic systems were studied by differential scan..." @default.
- W2895525880 created "2018-10-12" @default.
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- W2895525880 date "2018-10-01" @default.
- W2895525880 modified "2023-09-26" @default.
- W2895525880 title "Substituent Electronegativity and Isostructurality in the Polymorphism of Clonixin Analogues" @default.
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- W2895525880 doi "https://doi.org/10.1021/acs.cgd.8b01180" @default.
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