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• W2895542220 endingPage "34135" @default.
• W2895542220 startingPage "34126" @default.
• W2895542220 abstract "By milling 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane (CL-20) and hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) together, a nano CL-20/RDX co/mixed crystal explosive with a mean particle size of 141.6 nm is prepared from the raw materials, and the co/mixed crystals are characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman spectroscopy, infrared (IR) spectroscopy, X-ray photoelectron spectroscopy (XPS), differential scanning calorimetry (DSC) and thermal-infrared spectrometry online (DSC-IR) technology; furthermore, the impact, friction and thermal sensitivity of the samples are tested. The results show that after milling, the morphology of the co/mixed crystal explosive is near-spherical, and the particle size reveals a normal distribution. The milled sample showed the same molecular structure and surface elements as the raw materials, but the XRD test shows that CL-20/RDX has a new crystal phase and the Raman and IR spectra gave a supplementary confirmation for the existence of a cocrystal phase in the milled sample. The activation energy of the thermal decomposition of CL-20/RDX is 206.49 kJ mol-1 higher than that of raw RDX. DSC-IR analysis showed that the thermolysis of CL-20/RDX produces a large amount of CO2 and N2O and a small amount of H2O, NO2 and NO. The mechanical sensitivity of CL-20/RDX is very low. In impact sensitivity tests with a 5 kg hammer, the special height (H50) is 51.43 cm, which is higher than the values of 36.43 cm for raw CL-20 and 9.78 cm for raw RDX. In the friction sensitivity tests, the explosion probability (P) is 56%; however, the thermal sensitivity of CL-20/RDX is higher than that of the raw materials, with its 5 s burst point being only 243.51 °C." @default.
• W2895542220 created "2018-10-12" @default.
• W2895542220 creator A5000680684 @default.
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• W2895542220 date "2018-01-01" @default.
• W2895542220 modified "2023-10-12" @default.
• W2895542220 title "Mechanochemical fabrication and properties of CL-20/RDX nano co/mixed crystals" @default.
• W2895542220 cites W1763699740 @default.
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• W2895542220 doi "https://doi.org/10.1039/c8ra04122a" @default.
• W2895542220 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35548843" @default.
• W2895542220 hasPublicationYear "2018" @default.
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