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- W2895850280 abstract "Abstract The present work describes the synthesis of novel (E)-furan-2-yl(2-(2-hydroxybenzylidene)hydrazinyl) methaniminium in water/methanol(3:1) mixture, water acting as catalyst and also solvent to expedite reaction rate with high yield. In which, amine exchange and condensation reaction takes place between N-salicylidene aniline and furanoic acid hydrazide at one step. The structural characterization of prepared ligand was carried out by single crystal X-ray diffraction, elemental analysis and spectroscopy (UV–Vis, FT-IR and NMR) techniques. The single crystal X-ray diffraction result indicates that the ligand crystallizes in orthorhombic system with Pca21 space group. Further, Mn(II), Co(II), Ni(II), Cu(II), Zn(II) and Cd(II) complexes of ligand were prepared. Complexes were analyzed by elemental analysis, magnetic susceptibility and spectroscopy (UV–Vis, FT-IR and ESR) studies. The DNA binding studies of synthesized compounds were carried out and results suggest that, ligand L and its transition metal complexes 1–6 were binding to CT- DNA through intercalation. It was confirmed by intrinsic binding constant value in the order of 106 M−1. The fluorescence properties of ligand L and its metal complexes 1–6 were investigated; ligand showed broad emission spectra in the visible region and its metal complexes exhibited emission spectra in the blue to red." @default.
- W2895850280 created "2018-10-26" @default.
- W2895850280 creator A5043435774 @default.
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- W2895850280 date "2019-02-01" @default.
- W2895850280 modified "2023-10-18" @default.
- W2895850280 title "Facile synthesis, characterization, nucleic acid interaction and photoluminescent properties of (E)-furan-2-yl(2-(2-hydroxybenzylidene)hydrazinyl) methaniminium and its Mn(II), Co(II), Ni(II), Cu(II), Zn(II) and Cd(II) complexes" @default.
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- W2895850280 doi "https://doi.org/10.1016/j.molstruc.2018.10.037" @default.
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