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• W2895850730 abstract "The volatile methylisiloxanes (VMSs) D4, D5 and D6 have been included in the Candidate List of Substance of Very High Concern (SVHC) by European Chemicals Agency (ECHA) in June 2018. In response to the concerns from the recent SVHC, this study presents three pretreatment methods including purge and trap (P&T), solid-phase microextraction (SPME) and ultrasound-assisted solvent extraction (UASE) combined respectively with gas chromatography-mass spectrometry (GC-MS), for detection of 9 VMSs in food-contact silicone rubber products. Under their optimal operation conditions, three methods were validated. Compared with SPME-GC-MS and UASE-GC-MS, P&T-GC-MS method showed the lower method detection limits (8.40 × 10−4–1.95 × 10−3 mg/kg), the higher recoveries (91.05%–97.48%) and the good %RSD (7.6–11.9%). Considering to be of sensitivity, accuracy, stability, fully-automatic and solvent-free operation, P&T-GC-MS method was finally applied to quantify 9 VMSs in 56 commercial food-contact silicone rubber products. The results showed that 8 VMSs were found and their total contents varied from 17.97 mg/kg to 645.27 mg/kg in the 28 silicone rubber teats, meanwhile, D3, D4, D5 and D6 were detected and their total contents varied from 5.80 mg/kg to 1.45 × 103 mg/kg in the 28 pieces of silicone rubber bakeware." @default.
• W2895850730 created "2018-10-26" @default.
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• W2895850730 date "2019-02-01" @default.
• W2895850730 modified "2023-10-17" @default.
• W2895850730 title "Development, validation and comparison of three detection methods for 9 volatile methylsiloxanes in food-contact silicone rubber products" @default.
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• W2895850730 doi "https://doi.org/10.1016/j.polymertesting.2018.10.014" @default.
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