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- W2895854077 abstract "The rhodium catalyzed hydroformylation (oxo synthesis) of caryophyllene oxide (1) and β-caryophyllene (2), which are among the most abundant sesquiterpenic compounds in nature, leads to aldehydes with pleasant scents. The monoaldehydes derived from 1 and 2 were obtained in high yield under mild reaction conditions. A protocol for the efficient double-hydroformylation of 2 leading to a dialdehyde in a high yield is also described. Furthermore, these reactions can be efficiently carried out in the environmentally benign solvents: dimethylcarbonate, diethylcarbonate, 2-methyl-THF, and p-cymene, to replace conventional toluene and benzene. To the best of our knowledge, this is the first time that these solvents are employed in hydroformylation." @default.
- W2895854077 created "2018-10-26" @default.
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- W2895854077 date "2020-03-01" @default.
- W2895854077 modified "2023-09-27" @default.
- W2895854077 title "New scents using eco-friendly solvents: Oxo synthesis of aldehydes from caryophyllane sesquiterpenes" @default.
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- W2895854077 doi "https://doi.org/10.1016/j.cattod.2018.10.024" @default.
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