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• W2895884166 abstract "Photoelectrochemical (PEC) water splitting is an attractive technique to convert solar energy into chemical fuels of hydrogen and oxygen. Here, we report novel fabrication of Ta3N5 photoanodes using flux method. Layers of Ta3N5 with thickness of several hundred nanometers were grown on the surface of a Ta substrate by using a NaCl–Na2CO3 mixed flux for the crystal growth. The Ta substrate surface was dissolved by the heated and subsequently evaporated particles of NaCl–Na2CO3 in a flow of NH3, and Ta3N5 crystals were formed upon cooling. Analysis of the cross-sectional structure showed that the interface between the Ta3N5 film and the Ta substrate had few voids. In addition, the Ta3N5 film consisted of two layers—a sparse upper layer and a dense lower layer—at a holding temperature of 900 °C, which can be attributed to variations in the evaporation behavior of the flux under different fabrication conditions. When as-synthesized Ta3N5 crystal film was modified using Co–Pi as the co-catalyst, it exhibited an anodic photocurrent of 6.5 mA·cm–2 at 1.23 V vs a reversible hydrogen electrode. We also studied the formation process of the Ta3N5 crystal film and the role of NaCl and Na2CO3 used as the mixed flux by changing the holding temperature, holding time, and NaCl/Na2CO3 mixing ratio. Our results revealed that the thickness and structure of the Ta3N5 crystal film were controlled by these fabrication parameters." @default.
• W2895884166 created "2018-10-26" @default.
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• W2895884166 date "2018-10-10" @default.
• W2895884166 modified "2023-10-18" @default.
• W2895884166 title "Ta₃N₅ Photoanodes Fabricated by Providing NaCl–Na₂CO₃ Evaporants to Tantalum Substrate Surface under NH₃ Atmosphere" @default.
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• W2895884166 doi "https://doi.org/10.1021/acsaem.8b01162" @default.
• W2895884166 hasPublicationYear "2018" @default.
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