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- W2896433419 abstract "This work focuses on the process of polyazulene formation and investigates the morphology and electrochemical properties of synthesized materials. Polymeric materials were synthesized with different solvents under different conditions (stirring, concentration of the oxidizing agent, synthesis time). Polymers were formed from a solution containing azulene and FeCl3 as an oxidizing agent. Depending on the synthesis conditions, polyazulene could be changed from microstructures to spherical nanostructures. The size of these nanospheres could be controlled by the synthesis time, stirring medium and concentration of the oxidizing agent. Formation of a polymeric phase was confirmed by FT-IR and UV–vis spectroscopy. The obtained polymer was electrochemically active at a positive potential range due to the oxidation of azulene moieties. The voltammetric response corresponding to this electrochemical process depended on the synthesis conditions. In addition, the capacitance properties depended on the synthesis conditions due to differences in the surface morphologies obtained in different solvents used for polymerization. The highest capacitance of approximately 120 F g−1 was obtained for polyazulene nanoparticles." @default.
- W2896433419 created "2018-10-26" @default.
- W2896433419 creator A5019127564 @default.
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- W2896433419 date "2018-12-01" @default.
- W2896433419 modified "2023-09-26" @default.
- W2896433419 title "Chemically formed conducting polyazulene: From micro- to nanostructures" @default.
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- W2896433419 doi "https://doi.org/10.1016/j.synthmet.2018.10.002" @default.
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