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- W2896514316 abstract "A transition metal-free process has been reported for 1,2-dithiocyanation of alkynes in the presence of sodium persulfate and potassium thiocyanate reagent combination in a short reaction time under ambient air. Styrene derivatives are equally applicable under the same reaction conditions. Monothiocyanated vinyl derivatives were also synthesized from 2-ethynylpyridine and dimethyl acetylene dicarboxylate. The reaction proceeds by the radical/polar pathway as evidenced from our experiments and literature. After removal of the solvent from the reaction mixture by evaporation, the crude product was purified without conventional workup." @default.
- W2896514316 created "2018-10-26" @default.
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- W2896514316 date "2018-10-11" @default.
- W2896514316 modified "2023-09-27" @default.
- W2896514316 title "Mild, Efficient, and Metal-Free Radical 1,2-Dithiocyanation of Alkynes and Alkenes at Room Temperature" @default.
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- W2896514316 doi "https://doi.org/10.1021/acsomega.8b01762" @default.
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