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• W2896616001 abstract "A novel complex based on the Dawson-like [H 3 BiW 18 O 60 ] 6− , i.e. (C 2 H 9 N 2 ) 2 [{Cu(C 10 H 8 N 2 )(C 2 H 8 N 2 )} 2 (H 3 BiW 18 O 60 )]·5.5H 2 O or (enH) 2 [{Cu(2,2′-bipy)(en)} 2 (μ 4 -H 3 BiW 18 O 60 )]·5.5H 2 O, ( 1 ), where enH is protonated ethane-1,2-diamine, 2,2′-bipy is 2,2′-bipyridine and en is ethane-1,2-diamine, has been synthesized hydrothermally and characterized by elemental analysis, single-crystal X-ray diffraction analysis, IR spectroscopy, powder XRD, and thermogravimetry and differential thermal analysis (TG–DTA). For ( 1 ), each [H 3 BiW 18 O 60 ] 6− anion acts as a tetradentate ligand connecting [Cu(2,2′-bipy)(en)] 2+ fragments via two terminal and two bridging O atoms, forming a two-dimensional network structure. Along the a and c axes, polyoxometalate units are arranged in an AB … AB manner. The electrochemical behaviour of ( 1 )–CPE (CPE is a carbon paste electrode) was investigated in 2 M H 2 SO 4 solution by cyclic voltammetry (CV). The redox process of W VI/V takes place at E 1/2 = −0.58 (I–I′) and −0.37 V (II–II′), and at −0.04 V (III–III′) for Cu II/0 . The magnetic properties of ( 1 ) were investigated in the range 2–300 K and indicated the existence of strong antiferromagnetic exchange interactions between the Cu 2+ centres." @default.
• W2896616001 created "2018-10-26" @default.
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• W2896616001 date "2018-10-16" @default.
• W2896616001 modified "2023-10-09" @default.
• W2896616001 title "A novel two-dimensional layered Cu2+ complex based on Dawson-like [H3BiW18O60]6−: synthesis, structure and magnetic properties" @default.
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• W2896616001 doi "https://doi.org/10.1107/s205322961800935x" @default.
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• W2896616001 hasPublicationYear "2018" @default.
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