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• W2896669586 abstract "The oxonitridocarbidosilicates RE4Ba2[Si12O2N16C3]:Eu2+ (RE = Lu, Y) were synthesized by carbothermal reactions starting from RE2O3, graphite, Ba2Si5N8, Si(NH)2, and Eu2O3. The crystal structure of Lu4Ba2[Si12O2N16C3]:Eu2+ was elucidated on a submicron-sized single crystal by a combination of transmission electron microscopy and microfocused synchrotron radiation. The compound crystallizes in trigonal space group P3 (no. 143) with a = 16.297(4) Å, c = 6.001(2) Å, and Z = 3 (R1 = 0.0332, wR2 = 0.0834, GoF = 1.034). According to Rietveld refinements on powder X-ray diffraction data, Y4Ba2[Si12O2N16C3]:Eu2+ is isotypic with a = 16.41190(6) Å and c = 6.03909(3) Å. The crystal structures are built up of vertex-sharing SiC(O/N)3 tetrahedra forming star-shaped units [C[4](Si(O/N)3)4] with carbon atoms in fourfold bridging positions. Energy-dispersive X-ray spectroscopy and CHNS analysis correspond to the sum formula, lattice energy, and charge distribution calculations support the assignment of O/N/C atoms. When excited with UV to blue light, Eu2+-doped samples show green luminescence for RE = Lu (λem ≈ 538 nm, full width at half-maximum (fwhm) ≈ 3600 cm–1) and yellow emission in the case of RE = Y (λem ≈ 556 nm, fwhm ≈ 4085 cm–1)." @default.
• W2896669586 created "2018-10-26" @default.
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• W2896669586 date "2018-10-16" @default.
• W2896669586 modified "2023-09-30" @default.
• W2896669586 title "<i>RE</i>₄Ba₂[Si₁₂O₂N₁₆C₃]:Eu²⁺ (<i>RE</i> = Lu, Y): Green-Yellow Emitting Oxonitridocarbidosilicates with a Highly Condensed Network Structure Unraveled through Synchrotron Microdiffraction" @default.
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• W2896669586 doi "https://doi.org/10.1021/acs.inorgchem.8b02343" @default.
• W2896669586 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30351090" @default.
• W2896669586 hasPublicationYear "2018" @default.
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