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• W2896863986 startingPage "16475" @default.
• W2896863986 abstract "Abstract By reaction of alkali metal acetylides, A I C 2 H (A I =K, Rb, Cs), with elemental selenium in liquid ammonia highly crystalline powders of A I SeC 2 H were obtained. The structure analysis based on the resulting synchrotron powder diffraction data revealed that all compounds crystallize in an orthorhombic unit cell (Cmc2 1 , Z =4) exhibiting the elusive − SeC 2 H anion, which is unprecedented in a crystalline compound up to now. Elemental analysis and IR spectroscopic data confirm this finding. Upon heating, A I SeC 2 H compounds release acetylene based on DSC/TGA experiments resulting in powders with the proposed composition A I 2 Se 2 (C 2 ). The resulting powders were indexed with small cubic unit cells, but a reasonable structural model could not be developed up to now. Upon exposure of A I SeC 2 H compounds to water elemental selenium is formed again." @default.
• W2896863986 created "2018-10-26" @default.
• W2896863986 creator A5003067585 @default.
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• W2896863986 date "2018-11-12" @default.
• W2896863986 modified "2023-09-25" @default.
• W2896863986 title "A^ISeC₂H (A^I=K, Rb, Cs): Crystalline Compounds with the Elusive⁻Se-C≡C-H Anion" @default.
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• W2896863986 doi "https://doi.org/10.1002/anie.201810910" @default.
• W2896863986 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30347126" @default.
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