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• W2897051934 abstract "An ex-situ potentiometric titrations were normally performed using an oxidation/reduction potential (ORP) electrode to monitor the electrochemically generated active electron mediators, either oxidants or reductants, in a mediator generation plant. In the present investigation, an attempt was made to monitor electron mediator [Ni1+(CN)4]3- (Ni(I)) in-situ in a high electrolyte concentration (9 M KOH) during its electrochemical generation. A ring type flow cell developed using a 0.6 cm diameter electrode was tested on a standard redox couple of [Fe3+(CN)6]3- (Fe(III))/[Fe2+(CN)6]4- (Fe(II)) at different ratios during solution flow. The found results suggested that direct determination of an electrochemically prepared electron mediator is possible using a potentiometric method. A periodical potential change in the in-situ linear sweep voltammetry of electrogenerated Ni(I) during its electrochemical generation allowed the direct determination of electrogenerated Ni(I) by the ring type flow cell. A calibration plot derived from chemically synthesized Ni(I) using an ex-situ potentiometric titration or UV–visible spectra was used to monitor electrogenerated Ni(I) by the in-situ method. The electrochemically generated Ni(I) concentration detected in the 0–4.5 mmol/L region that followed non-Nernstian behavior. A change in the Ni(I) concentration during N2O removal at the scrubber column suggesting that air pollutant removal can be monitored using the in-situ flow sensor cell, once how many electron involved in the removal process." @default.
• W2897051934 created "2018-10-26" @default.
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• W2897051934 date "2019-02-01" @default.
• W2897051934 modified "2023-09-27" @default.
• W2897051934 title "Real time potentiometric macro flow sensor: An innovative tool to monitor electrogenerated electron mediator in high concentrated electrolyte during electrolysis and air pollutants removal" @default.
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• W2897051934 doi "https://doi.org/10.1016/j.electacta.2018.10.118" @default.
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