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• W2897536897 abstract "Precise research on the RbF–Al2O3 system was carried out by means of combining X-ray powder diffraction, high-field solid-state NMR spectroscopy, and thermal analysis methods. α-Rb3AlF6, RbAlO2, Rb2Al22O34, and new phase, Rb2Al2O3F2, were identified in the system. The structure of this new rubidium oxofluoroaluminate was determined. It is built up from single layers of oxygen-connected AlO3F tetrahedra, those layers beeing separated by fluorine atoms. This type of structure exhibits a decent ionic conductivity at ambient temperature, 1.74 × 10–6 S cm–1. The similar structural arrangement of O3Al–O–AlO3 and FO2Al–O–AlO2F tetrahedra of the conduction planes in Rb2Al22O34 and Rb2Al2O3F2 were confirmed by 27Al NMR measurements. A thermal analysis of the RbF–Al2O3 system revealed that it can be defined as a pseudobinary subsystem of the more general quaternary RbF–AlF3–Al2O3–Rb2O phase diagram. From a phase analysis of individual phase fields, the mutual metastable behavior of all founded phases can be considered. It was observed that fluoro- and oxoaluminates exist together. Rb2Al2O3F2 is more stable under high temperature. Rubidium fluoro- and oxoaluminates are metastable precursors of the thermodynamically more stable structure of rubidium oxofluoroaluminate." @default.
• W2897536897 created "2018-10-26" @default.
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• W2897536897 date "2018-10-24" @default.
• W2897536897 modified "2023-10-16" @default.
• W2897536897 title "Oxo- and Oxofluoroaluminates in the RbF–Al₂O₃ System: Synthesis and Structural Characterization" @default.
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• W2897536897 doi "https://doi.org/10.1021/acs.inorgchem.8b02275" @default.
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• W2897536897 hasPublicationYear "2018" @default.
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