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- W2897555180 abstract "Azide–alkyne “click” cyclization was used to prepare a series of polymerizable acetoacetate monomers containing a 1,2,3-trizolium ionic liquid group. The monomers were subsequently polymerized using base-catalyzed Michael addition chemistry, producing a series of covalently crosslinked 1,2,3-triazolium poly(ionic liquid) (TPIL) networks. Structure–activity relationships were conducted to gauge how synthetic variables, such as counteranion ([Br], [NO3], [BF4], [OTf], and [NTf2]), and crosslink density (acrylate/acetoacetate ratio) effected thermal, mechanical, and conductive properties. TPIL networks were found to exhibit ionic conductivities in the range of 10–6–10–9 S/cm (30 °C, 30% relative humidity), as determined from dielectric relaxation spectroscopy, despite their highly crosslinked nature. Temperature-dependent conductivities demonstrate a dependence on polymer glass transition, with free-ion concentrations impacted by various ions’ Lewis acidity/basicity and ion mobilities impacted by freely mobile anion size." @default.
- W2897555180 created "2018-10-26" @default.
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- W2897555180 date "2018-10-18" @default.
- W2897555180 modified "2023-10-14" @default.
- W2897555180 title "Covalently Crosslinked 1,2,3-Triazolium-Containing Polyester Networks: Thermal, Mechanical, and Conductive Properties" @default.
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- W2897555180 doi "https://doi.org/10.1021/acsomega.8b01949" @default.
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