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- W2897557953 abstract "[23743-26-2] C26H48P2 (MW 422.62) 1S/C26H48P2/c1-5-13-23(14-6-1)27(24-15-7-2-8-16-24)21-22-28(25-17-9-3-10-18-25)26-19-11-4-12-20-26/h23-26H,1-22H2 BOUYBUIVMHNXQB-UHFFFAOYSA-N (ligand for metal-catalyzed reactions) Alternate Names: 1,2-ethanediylbis[dicyclohexyl]phosphine, ethylenebis(dicyclohexylphosphine), dcpe, dCype. Physical Data: mp 96–97 °C. Form Supplied in: white to off-white crystal or powder. Purification: sublimation at 135 °C/0.06 mm.1 Preparative Method: the title compound is prepared by addition of ethylene glycol over chlorodicyclohexylphosphane. The resulting intermediate was heated to give the corresponding bis phosphine oxide, which is reduced by trichlorosilane. Handling, Storage, and Precautions: may be harmful if inhaled. Causes respiratory tract irritation. May be harmful if absorbed through skin. Causes skin and eye irritation. May be harmful if swallowed. The toxicity of this reagent is not known; therefore, it should be manipulated in a well-ventilated fume hood. Protective gloves, clothing, and eye/face protection should be worn while manipulating this reagent. Keep container tightly closed in a dry and well-ventilated place. Moisture sensitive. Handle and store under inert gas preferentially." @default.
- W2897557953 created "2018-10-26" @default.
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- W2897557953 date "2017-04-10" @default.
- W2897557953 modified "2023-10-01" @default.
- W2897557953 title "1,2-Bis(dicyclohexylphosphino)ethane" @default.
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