FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2897850221> ?p ?o ?g. }

• W2897850221 endingPage "279" @default.
• W2897850221 startingPage "272" @default.
• W2897850221 abstract "Two pairs of homoisoflavonoid analogues, 6-aldehydo-isoophiopogonanone A (1) / 6-aldehydo-isoophiopogonanone B (2) and methylophiopogonanone A (3) / methylophiopogonanone B (4), were obtained from the fibrous roots of Ophiopogon japonicus (L. f.) Ker-Gawl. (FROJ) by silica gel column chromatography (SGCC) and recycling high-speed counter-current chromatography (rHSCCC). First, the ethyl acetate fraction from the 70% ethanol extract was pre-separated by SGCC with a petroleum ether–ethyl acetate gradient (50:1–2:1, v/v). Then, the two sub-fractions containing homoisoflavonoid analogues were further separated by rHSCCC with n-hexane–ethyl acetate–methanol–acetonitrile–water (3:2:3.5:1:0.5, v/v) and n-hexane–ethyl acetate–methanol–acetonitrile–water (3:2:2.5:1:1.5, v/v). Finally, 6-aldehydo-isoophiopogonone A (16 mg), 6-aldehydo-isoophiopogonanone B (26 mg), methylophiopogonanone A (46 mg), and methylophiopogonanone B (148 mg) were obtained with purities of 97.82%, 96.70%, 97.76%, and 94.62%. Their structures were identified by high-resolution quadrupole-time-of-flight mass spectrometry (HR-QTOF-MS), ultraviolet (UV), and nuclear magnetic resonance spectroscopy (1H-NMR and 13C-NMR). These results demonstrated that rHSCCC could be used for the large scale preparation of homoisoflavonoid analogues from FROJ, which provides scientific support for utilization of untraditional medicinal part of O. japonicus and also for reduction in waste of plant resources. Additionally, an online antioxidant activity assay was investigated with hyphenated HSCCC-DPPH (1-diphenyl-2-picrylhydrazyl) radical scavenging detection." @default.
• W2897850221 created "2018-10-26" @default.
• W2897850221 creator A5006506850 @default.
• W2897850221 creator A5007195649 @default.
• W2897850221 creator A5065925045 @default.
• W2897850221 creator A5073181406 @default.
• W2897850221 creator A5075140188 @default.
• W2897850221 creator A5085372235 @default.
• W2897850221 date "2019-12-01" @default.
• W2897850221 modified "2023-09-23" @default.
• W2897850221 title "Isolation of homoisoflavonoids from the fibrous roots of <i>Ophiopogon japonicus</i> by recycling high-speed counter-current chromatography and online antioxidant activity assay" @default.
• W2897850221 cites W1528267482 @default.
• W2897850221 cites W1835014067 @default.
• W2897850221 cites W1966742639 @default.
• W2897850221 cites W1966987177 @default.
• W2897850221 cites W1981636492 @default.
• W2897850221 cites W1988068739 @default.
• W2897850221 cites W1999737354 @default.
• W2897850221 cites W2001876914 @default.
• W2897850221 cites W2001893482 @default.
• W2897850221 cites W2018756020 @default.
• W2897850221 cites W2026185011 @default.
• W2897850221 cites W2026378194 @default.
• W2897850221 cites W2026631712 @default.
• W2897850221 cites W2035233783 @default.
• W2897850221 cites W2037006503 @default.
• W2897850221 cites W2040582759 @default.
• W2897850221 cites W2041412612 @default.
• W2897850221 cites W2050725484 @default.
• W2897850221 cites W2067978637 @default.
• W2897850221 cites W2074270865 @default.
• W2897850221 cites W2077759081 @default.
• W2897850221 cites W2079426550 @default.
• W2897850221 cites W2110644172 @default.
• W2897850221 cites W2134664574 @default.
• W2897850221 cites W2142138065 @default.
• W2897850221 cites W2150589107 @default.
• W2897850221 cites W2275401450 @default.
• W2897850221 cites W2301314732 @default.
• W2897850221 cites W2312611000 @default.
• W2897850221 cites W2318610990 @default.
• W2897850221 cites W2401136691 @default.
• W2897850221 cites W2568049037 @default.
• W2897850221 cites W2584054527 @default.
• W2897850221 cites W2586209421 @default.
• W2897850221 cites W3141049144 @default.
• W2897850221 cites W4245444487 @default.
• W2897850221 doi "https://doi.org/10.1556/1326.2018.00509" @default.
• W2897850221 hasPublicationYear "2019" @default.
• W2897850221 type Work @default.
• W2897850221 sameAs 2897850221 @default.
• W2897850221 citedByCount "8" @default.
• W2897850221 countsByYear W28978502212019 @default.
• W2897850221 countsByYear W28978502212021 @default.
• W2897850221 countsByYear W28978502212022 @default.
• W2897850221 countsByYear W28978502212023 @default.
• W2897850221 crossrefType "journal-article" @default.
• W2897850221 hasAuthorship W2897850221A5006506850 @default.
• W2897850221 hasAuthorship W2897850221A5007195649 @default.
• W2897850221 hasAuthorship W2897850221A5065925045 @default.
• W2897850221 hasAuthorship W2897850221A5073181406 @default.
• W2897850221 hasAuthorship W2897850221A5075140188 @default.
• W2897850221 hasAuthorship W2897850221A5085372235 @default.
• W2897850221 hasBestOaLocation W28978502211 @default.
• W2897850221 hasConcept C178790620 @default.
• W2897850221 hasConcept C185592680 @default.
• W2897850221 hasConcept C2776148806 @default.
• W2897850221 hasConcept C2777463227 @default.
• W2897850221 hasConcept C2778004101 @default.
• W2897850221 hasConcept C2779532046 @default.
• W2897850221 hasConcept C2779607525 @default.
• W2897850221 hasConcept C2779858419 @default.
• W2897850221 hasConcept C2781401929 @default.
• W2897850221 hasConcept C43617362 @default.
• W2897850221 hasConcept C4725764 @default.
• W2897850221 hasConcept C51724486 @default.
• W2897850221 hasConcept C63258622 @default.
• W2897850221 hasConceptScore W2897850221C178790620 @default.
• W2897850221 hasConceptScore W2897850221C185592680 @default.
• W2897850221 hasConceptScore W2897850221C2776148806 @default.
• W2897850221 hasConceptScore W2897850221C2777463227 @default.
• W2897850221 hasConceptScore W2897850221C2778004101 @default.
• W2897850221 hasConceptScore W2897850221C2779532046 @default.
• W2897850221 hasConceptScore W2897850221C2779607525 @default.
• W2897850221 hasConceptScore W2897850221C2779858419 @default.
• W2897850221 hasConceptScore W2897850221C2781401929 @default.
• W2897850221 hasConceptScore W2897850221C43617362 @default.
• W2897850221 hasConceptScore W2897850221C4725764 @default.
• W2897850221 hasConceptScore W2897850221C51724486 @default.
• W2897850221 hasConceptScore W2897850221C63258622 @default.
• W2897850221 hasIssue "4" @default.
• W2897850221 hasLocation W28978502211 @default.
• W2897850221 hasOpenAccess W2897850221 @default.
• W2897850221 hasPrimaryLocation W28978502211 @default.
• W2897850221 hasRelatedWork W2036115817 @default.
• W2897850221 hasRelatedWork W2045511210 @default.
• W2897850221 hasRelatedWork W2083905271 @default.
• W2897850221 hasRelatedWork W2087631576 @default.

• next