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• W2897851080 abstract "Abstract Crystalline bis‐ N ‐alkyl‐chlorotriazines 2 – 6 can be considered multilayers of lipid bilayers comprising a rigid hydrogen‐bonded tape in the polar layer separated by a lipid region of small to medium‐length alkyl chains. The persistent ordering of these tapes acts as a scaffold in the solid state enabling measurement of temperature‐induced conformational changes in the “lipid phase” using X‐ray crystallography. The alkyl chains in these structures are loosely packed but generally ordered at low temperature, undergoing a slow transition to a disordered structure clearly observed in the Raman spectrum. The longer‐chain derivatives 4 – 6 show a distinct Raman spectrum for the ordered and disordered crystallographic phases enabling a least squares fitting at each temperature point. Calibration of the Raman fit values for 5 and 6 using powder X‐ray diffraction allows a quantification of each phase and highlights the unique response of each derivative with temperature. This approach for quantifying the onset of disorder and structural phase transitions should be relevant to a wide range of lipid‐based systems." @default.
• W2897851080 created "2018-10-26" @default.
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• W2897851080 date "2018-10-11" @default.
• W2897851080 modified "2023-10-05" @default.
• W2897851080 title "Quantifying alkyl chain disorder in crystalline models of lipid bilayers using Raman spectroscopy" @default.
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• W2897851080 doi "https://doi.org/10.1002/jrs.5501" @default.
• W2897851080 hasPublicationYear "2018" @default.
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