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• W2897979661 abstract "The synthesis of a 6-CF3-substituted 2-amino-dihydro-1,3-thiazine via N,N-diethylaminosulfur trifluoride (DAST)-mediated cyclization of N-hydroxypropyl thiourea 6 is described. This reaction gave 6-CF3-1,3-thiazine 7 with high chemical yield and chemoselectivity, suppressing the common byproduct of oxazine 8. This new protocol enabled access to 6-CF3-substituted 1,3-thiazine β-secretase inhibitor 2." @default.
• W2897979661 created "2018-10-26" @default.
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• W2897979661 date "2018-10-12" @default.
• W2897979661 modified "2023-09-28" @default.
• W2897979661 title "Synthesis of a 6-CF₃-Substituted 2-Amino-dihydro-1,3-thiazine β-Secretase Inhibitor by <i>N</i>,<i>N</i>-Diethylaminosulfur Trifluoride-Mediated Chemoselective Cyclization" @default.
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• W2897979661 doi "https://doi.org/10.1021/acs.joc.8b02179" @default.
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