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- W2898061639 abstract "The free water in calcined phyllosilicate–water mixtures exhibits a distinctly different behaviour in its X-ray amorphous scattering contribution as opposed to fly ash– or limestone powder–water mixtures. While fly ash and limestone powder yield a continuous increase in the scattering contribution when water is added, the scattering contribution stagnates for calcined phyllosilicates over a wide range of water addition. There is a direct correlation between the consistency of the sample and the X-ray amorphous scattering contribution caused by the water. The same correlation can also be found in in situ X-ray diffraction measurements of hydrating systems. As long as the sample has a pasty consistency, the scattering contribution of the water decreases with progressive reaction. After the transition from fresh paste to final set, there is no further reduction of the X-ray amorphous scattering contribution caused by the free water, which means that the free water cannot be quantified correctly from this point in time." @default.
- W2898061639 created "2018-10-26" @default.
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- W2898061639 date "2018-10-11" @default.
- W2898061639 modified "2023-10-16" @default.
- W2898061639 title "Quantitative X-ray diffraction of free, not chemically bound water with the PONKCS method" @default.
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- W2898061639 doi "https://doi.org/10.1107/s1600576718012888" @default.
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