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• W2898080903 abstract "As an extension of our continued interest in the preparation of inorganic–organic hybrids, we report the successful hydrothermal synthesis of sodium tris[triaqua(μ-1,10-phenanthroline-2,9-dicarboxylato)dysprosium(III)] silicododecatungstate dodecahydrate, {[DyNa(C 14 H 6 N 2 O 4 ) 3 (H 2 O) 9 (SiW 12 O 40 )]·12H 2 O} n or Na[Dy(PDA)(H 2 O) 3 ] 3 [SiW 12 O 40 ]·12H 2 O ( 1 ), and sodium aqua tris[tetraaqua(μ-4-hydroxypyridine-2,6-dicarboxylato)praseodymium(III)] silicododecatungstate dodecahydrate, {[NaPr(C 7 H 3 NO 5 ) 3 (H 2 O) 13 (SiW 12 O 40 )]·12H 2 O} n or Na(H 2 O)[Pr(pydc-OH)(H 2 O) 4 ] 3 [SiW 12 O 40 ]·12H 2 O ( 2 ) (in which H 2 PDA is 1,10-phenanthroline-2,9-dicarboxylic acid and H 2 pydc-OH is 4-hydroxypyridine-2,6-dicarboxylic acid or chelidamic acid). Both compounds have been characterized using elemental analysis, IR spectroscopy and X-ray diffraction methods. Structural characterization by single-crystal X-ray diffraction reveals that these compounds consist of [SiW 12 O 40 ] 4− Keggin-type polyoxometalates (POMs), where a single {W 3 O 13 } triad is decorated with a trinuclear Ln complex. Moreover, the decorated polyanions are involved in a series of intermolecular interactions, such as hydrogen bonds and anion–π interactions, resulting in three-dimensional supramolecular architectures. Density functional theory (DFT) studies were conducted to support these intermolecular interactions in both 1 and 2 , and have been rationalized using molecular electrostatic potential (MEP) surface calculations." @default.
• W2898080903 created "2018-10-26" @default.
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• W2898080903 date "2018-10-17" @default.
• W2898080903 modified "2023-10-16" @default.
• W2898080903 title "Surface-grafted lanthanoid complexes of the tungstosilicate polyanion [SiW₁₂O₄₀]⁴⁻: a synthetic, structural and computational investigation" @default.
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• W2898080903 doi "https://doi.org/10.1107/s2053229618009580" @default.
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