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• W2898461687 abstract "Abstract In this work we present a unique method to synthesize χ‐Al 2 O 3 and α‐Al 2 O 3 doped with Cr 3+ (ruby). The ruby is synthesized by mechanical milling of pseudoboehmite that is doped in‐situ with chromium. The doping is carried by adding chromium sulfate hydrate to an aqueous solution rich in aluminum sulfate hydrate. The pH in the solution is controlled to be between 9 and 10 by using ammonia, which induces the pseudoboehmite precipitation. The Cr 3+ is added for its remarkable effects on the detectability of ruby emitting luminescent R 1 and R 2 bands that are traceable in Raman spectroscopy. The formation of ruby is detected at milling times as short as 5 hours and increased with the milling time. Ruby phase is further confirmed by means of true atomic resolution Transmission Electron Microscopy ( TEM )." @default.
• W2898461687 created "2018-11-02" @default.
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• W2898461687 date "2018-11-05" @default.
• W2898461687 modified "2023-10-18" @default.
• W2898461687 title "Mechanochemical synthesis of α‐Al ₂ O ₃ ‐Cr ³⁺ (Ruby) and χ‐Al ₂ O ₃" @default.
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• W2898461687 doi "https://doi.org/10.1111/jace.16171" @default.
• W2898461687 hasPublicationYear "2018" @default.
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